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Beilstein J. Org. Chem. 2018, 14, 2220–2228, doi:10.3762/bjoc.14.196
Graphical Abstract
Figure 1: Continuous-flow process to produce and react N-chloramines.
Figure 2: Left: Laboratory scale CSTR developed by our group [8]. Right: 5-stage CSTR configuration using co-fee...
Figure 3: Continuous-flow amide 18 formation using 1-stage CSTR. Blue squares: FeCl3 included; red circles: F...
Scheme 1: Continuous-flow transfer hydrogenation of in situ generated imines.
Beilstein J. Org. Chem. 2016, 12, 2019–2025, doi:10.3762/bjoc.12.189
Scheme 1: Functionalised CBTs 1 can be used for the synthesis of luciferins 3 and for bioorthogonal ligations...
Scheme 2: Reported synthetic routes to ACBT 8: A) Original route reported by Takakura et al. [14] and Wang et al. ...
Figure 1: Calorimeter traces for the addition of aqueous NaCN (A) or water (B) to a solution of 6 and DABCO i...
Scheme 3: Scale-up of ACBT synthesis.
Beilstein J. Org. Chem. 2015, 11, 2408–2417, doi:10.3762/bjoc.11.262
Scheme 1: Two-phase reaction of N,N-dialkylamine and sodium hypochlorite.
Figure 1: Calorimeter trace for the single phase reaction of morpholine (aq) and NaOCl (aq). Q Comp: compensa...
Figure 2: Meso-scale static mixer set-up for continuous N-chloramine formation. (a) Pumps, (b) reagent soluti...
Figure 3: Effect of static mixers on biphasic solution.
Figure 4: Progress of reaction for continuous formation of N-chloromorpholine. Morpholine (toluene) 0.9 M 1 m...
Figure 5: CSTR set-up for N-chloramine formation. (a) Syringe pump, (b) collection vessels, (c) reactor (50 m...
Figure 6: Interior of 50 mL CSTR.